Mimar Sinan Güzel Sanatlar Üniversitesi Açık Bilim, Sanat Arşivi

Açık Bilim, Sanat Arşivi, Mimar Sinan Güzel Sanatlar Üniversitesi tarafından doğrudan ve dolaylı olarak yayınlanan; kitap, makale, tez, bildiri, rapor gibi tüm akademik kaynakları uluslararası standartlarda dijital ortamda depolar, Üniversitenin akademik performansını izlemeye aracılık eder, kaynakları uzun süreli saklar ve yayınların etkisini artırmak için telif haklarına uygun olarak Açık Erişime sunar.

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A sensitive analytical method for the determination of copper at trace levels with Sb2O4 nanoparticles based dispersive solid phase extraction

dc.contributor.authorSerbest, Hakan
dc.contributor.authorBakirdere, Sezgin
dc.date.accessioned2025-10-08T13:19:49Z
dc.date.available2025-10-08T13:19:49Z
dc.date.issued2025en_US
dc.identifier.citationSerbest, H., & Bakirdere, S. (2025). A sensitive analytical method for the determination of copper at trace levels with Sb2O4 nanoparticles based dispersive solid phase extraction. Journal of the Indian Chemical Society, 102(11), 102103. https://doi.org/10.1016/J.JICS.2025.102103en_US
dc.identifier.issn0019-4522
dc.identifier.urihttps://doi.org/10.1016/J.JICS.2025.102103
dc.identifier.urihttps://hdl.handle.net/20.500.14124/10155
dc.description.abstractThis study presents antimony oxide nanoparticles (AO-NPs)-based dispersive solid phase extraction (DSPE) method for the determination of copper ions in lavender tea matrices with high sensitivity and accuracy at trace levels by flame atomic absorption spectrometry (FAAS) system. AO-NPs used as sorbent material were produced by microwave-assisted synthesis method by setting a defined temperature program. Limit of detection (LOD) value was calculated as 0.41 μg L−1 under optimal operating conditions. Linearity was obtained in the range of 2.5–40 μg L−1. Increase in detection power/sensitivity were calculated based on LOD values of FAAS and AO-NP-DSPE-FAAS systems and the slopes of the calibration plot equations and were found to be 169.4 and 123.1, respectively. The recovery results in lavender tea matrices recorded in the range of 103 %–118.2 % by employing the matrix matching calibration strategy indicated that the presented method is feasible for lavender tea and similar matrices.en_US
dc.language.isoengen_US
dc.publisherElsevieren_US
dc.relation.ispartofJournal of the Indian Chemical Societyen_US
dc.rightsinfo:eu-repo/semantics/restrictedAccessen_US
dc.subjectCopperen_US
dc.subjectAntimony oxide nanoparticlesen_US
dc.subjectMicrowave synthesisen_US
dc.subjectFlame atomic absorption spectrometryen_US
dc.titleA sensitive analytical method for the determination of copper at trace levels with Sb2O4 nanoparticles based dispersive solid phase extractionen_US
dc.typearticleen_US
dc.authorid0000-0003-2303-0408en_US
dc.departmentYüksekokullar, Kültür Varlıkları Koruma ve Onarım Yüksekokulu, Kültür Varlıklarını Koruma ve Onarım Bölümüen_US
dc.institutionauthorSerbest, Hakan
dc.identifier.doi10.1016/j.jics.2025.102103en_US
dc.identifier.volume102en_US
dc.identifier.issue11en_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.authorwosidCAG-6203-2022en_US
dc.authorscopusid57190251193en_US
dc.identifier.wosqualityQ2en_US
dc.identifier.wosWOS:001572155900001en_US
dc.identifier.scopus2-s2.0-105015423475en_US


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